Hexarelin Technical Specification Sheet

Molecular Properties

Parameter Value
Chemical Name Hexarelin / Examorelin
Amino Acid Sequence His-D-2-Methyl-Trp-Ala-Trp-D-Phe-Lys-NH₂
Molecular Formula C₄₇H₅₈N₁₂O₆
Molecular Weight 887.04 g/mol
CAS Number 140703-51-1
Sequence Length 6 amino acids (synthetic hexapeptide with D-amino acids and methylation)
Receptor Target Growth Hormone Secretagogue Receptor 1a (GHS-R1a) / Ghrelin receptor; CD36

Physical Properties

Property Specification
Appearance White to off-white lyophilized powder
Solubility Soluble in water or bacteriostatic water at ≥1 mg/mL; pH 5.0-7.0
pH (1% solution) 5.0 - 7.0
Hygroscopicity Low to moderate; standard desiccated storage
Solution Stability Stable at 4°C for 10-14 days; enhanced stability from D-amino acids and methylation

Analytical Specifications

Test Specification
HPLC Purity ≥98.0%
Mass Spectrometry Confirmed [M+H]⁺ = 887.04 ± 0.5 Da
Peptide Content ≥95% (by amino acid analysis)
Endotoxin Level <1.0 EU/mg
Acetate Content ≤5%
TFA Content ≤0.1%
Water Content ≤6% (Karl Fischer)

Storage Parameters

Condition Specification
Lyophilized Storage -20°C, desiccated, protected from light
Lyophilized Shelf Life 24-36 months when stored properly
Reconstituted Storage 2-8°C for up to 14 days; -20°C for up to 3 months
Reconstitution Protocol Add 1-2 mL sterile water or bacteriostatic water to 5 mg vial; gentle vortex 30 seconds
Freeze-Thaw Cycles Tolerates up to 5 cycles; superior stability vs unmodified peptides
Light Sensitivity Moderate; store in amber vials recommended

Research Dosing Reference

Application Typical Dose Range Frequency Route
In Vitro Pituitary Cell Assays 1-500 nM Acute stimulation (30 min to 2 hours) Culture media
Small Animal Models (Rodent) 50-300 μg/kg 1-2x daily SC, IV, or oral
GH Secretion Studies 100-200 μg/kg Single dose or BID for 7-28 days SC preferred
Cardioprotection Research 80-160 μg/kg Daily or BID for 1-4 weeks SC or IV
Note: Dosing information is for research reference only. Hexarelin is intended for laboratory research. Most potent GHRP for GH release; notable cardioprotective effects.

Key Research Studies

Year Study Focus Key Findings
1995 Discovery and potency characterization 2-methyl-D-Trp modification at position 2 increased GH-releasing potency 5-10x vs GHRP-6; demonstrated EC₅₀ of 0.05-0.5 nM (most potent synthetic GHRP); maintained stability and oral bioactivity
2000 Cardioprotective effects in ischemia models Hexarelin (80 μg/kg BID) reduced myocardial infarct size by 40-50%; effects partly GHS-R1a-independent; identified CD36 receptor interaction mediating cardiac protection
2006 Multi-organ protective effects Chronic hexarelin administration protected heart, kidney, liver from ischemia-reperfusion injury; anti-apoptotic effects via CD36 activation; reduced inflammatory cytokines 30-50%; GH-independent mechanisms identified
2011 Cortisol and prolactin co-secretion Hexarelin stimulation increased cortisol 2-3x and prolactin 3-5x alongside GH release; greatest ACTH/cortisol stimulation among GHRPs; limits therapeutic application but valuable research tool

Mechanism of Action

Biological Pathway Description
GHS-R1a Activation Most potent GHS-R1a agonist (Kd ~0.1-1 nM); 5-10x more potent than GHRP-6 for GH release; stimulates pituitary somatotrophs and hypothalamic GHRH neurons
GH/ACTH/Prolactin Secretion Strongest GH release among GHRPs; significant ACTH/cortisol co-stimulation (2-3x baseline); prolactin elevation (3-5x); peak GH at 15-30 minutes post-dose
CD36 Receptor Activation Binds CD36 (fatty acid translocase) with moderate affinity; mediates cardioprotection, anti-inflammatory effects, and anti-apoptotic actions independent of GH
Cardioprotection Direct cardiac effects via CD36; reduces oxidative stress; inhibits apoptosis; improves post-ischemic recovery; preserves contractile function
Half-Life 30-70 minutes (IV/SC); 2-methyl modification increases stability; oral bioavailability 5-10% (unusual for peptides)

Comparative Analysis: Hexarelin Potency

Compound GH Release EC₅₀ Relative Potency ACTH/Cortisol Effect
Hexarelin 0.05-0.5 nM 10x (reference) Strong (2-3x)
GHRP-2 0.1-1 nM 5-8x Moderate (1.5-2x)
GHRP-6 0.2-2 nM 5x Moderate (1.5-2x)
Ipamorelin 1-10 nM 1x Minimal (no increase)
GHRH 0.5-2 nM 1-2x None

Quality Control Parameters

Test Method Acceptance Criteria
Appearance (visual) White to off-white powder; no discoloration
2-Methyl-D-Trp Verification Position 2 modification confirmed by MS/MS; methylation >98%
Chiral Purity D-amino acids at positions 2 and 5 confirmed; >98% stereochemical purity
RP-HPLC (purity) Main peak ≥98.0%; no single impurity >0.5%
ESI-MS (identity) [M+H]⁺ = 887.04 ± 0.5 Da confirmed
Biological Activity ≥90% potency vs reference in GH release assay

Structure-Activity Relationship

Position Amino Acid Structural Role
1 L-His N-terminal; imidazole ring; similar to GHRP-6
2 D-2-Methyl-Trp KEY MODIFICATION: 2-methyl group increases potency 5-10x; D-configuration essential; enhanced receptor binding
3 L-Ala Conformational spacer
4 L-Trp Essential for GHS-R1a activation; indole ring critical
5 D-Phe Receptor selectivity; D-configuration prevents degradation
6 L-Lys-NH₂ C-terminal; positive charge; amidation required

Reported Biological Effects

Effect Category Observed Changes Timeframe
GH Secretion Peak GH increase 10-30x baseline (highest in GHRP class); occurs 15-30 min post-dose Acute (15-60 minutes)
ACTH/Cortisol Increased ACTH 2-3x, cortisol 2-3x (strongest among GHRPs); limits chronic use Acute (30-90 minutes)
Prolactin Elevated 3-5x baseline; dose-dependent response Acute (30-120 minutes)
Cardioprotection Reduced infarct size 40-50%; improved ejection fraction; anti-apoptotic effects Hours to days
Appetite Moderate increase (+20-40%); less than GHRP-6 but present 1-3 hours

External References

1. Bowers CY. Unnatural growth hormone-releasing peptide begets natural ghrelin. J Clin Endocrinol Metab. 2001;86(4):1464-9. https://academic.oup.com/jcem/article/86/4/1464/2849229

2. Muccioli G, et al. Growth hormone-releasing peptides and the cardiovascular system. Ann Endocrinol (Paris). 2000;61(1):27-31. https://pubmed.ncbi.nlm.nih.gov/10790589/

3. National Center for Biotechnology Information. PubChem Compound Summary for Hexarelin. https://pubchem.ncbi.nlm.nih.gov/compound/Hexarelin

Disclaimer: This product is intended for research use only. Not for human or veterinary diagnostic or therapeutic use. Hexarelin is the most potent GHRP but also stimulates ACTH/cortisol significantly.